
First draft presented to Linda Moulton Howe 07 August 1996
Nicholas A. Reiter Updated November 30, 2001
The following report appears here for the first time, at least in it's original form. It
represents a most interesting adventure in the realm of UFO detective work. Some readers may recall the on-going
debate on the Art Bell show back in 1996 and 1997 relating to the claimed fragment of the crashed Roswell saucer.
Research into the claimed artifact was hosted and managed by author and UFO personality Linda Moulton Howe. Linda
had partitioned the fragment presented to Art Bell into smaller sections that were then analyzed at assorted labs
around the country. NR was one of the chosen. As the reader will see, we had a bit of a leg up on this one.
The metal sample was eventually returned to Linda Howe, though we retain a very tiny fragment to
this day, with her permission. While our analysis of the sample by SEM and EDS spectroscopy agreed with that
performed at the other labs, our opinion of the origin of the sample did not represent the final "verdict" that
appeared to win out on Art Bell's show, or later literary references. We were, and remain, skeptical for reasons
that will become apparent. Following the text of the report is a short update. Read on, and remember that nothing
is as it seems...
I. Overview
On 12 July, 1996, I received by Fed Ex a small metal artifact from LMH. The purported origin of
this piece, as well as highlights of previous analytical work, had been revealed to me by LMH in earlier telephone
conversations. Along with the artifact portion, I received several color photographs of the parent artifact, as
well as some SEM photos, and a written summary of previous EDS and SIMS work. After personal viewing by me, the
original photos were sent back to LMH.
From 12 July to the present, I have performed numerous simple tests and analytical operations on
the sample. The results of these tests, to date, are summarized here.
II. Physical Characteristics
The artifact appears to be a small chunk of lightweight metal, sawed or micro-tomed from a larger
parent piece. It is irregular in contour, and measured (as received) about 22mm x 4mm x 6mm. Of the two non-cut
sides, one is of a silvery colour, textured with many small convex "bumps". The other side is of a gold- black
colour, with a fluted surface; a concave "negative" of the silvery side topography. Upon handling, a thin (about
1mm thick) portion delaminated from the original piece. This smaller portion broke away along a line following the
contour of the primary piece. The smaller portion retained the characteristics of silvery and blackish sides, with
the now exposed surface of the large portion being silvery - convex. The smaller fragment was reserved for
destructive testing.
Initial visual inspection, along with inspection of the photos of the parent artifact, shows a
clear columnar structure along with discrete bands or layers. The artifact, overall, appears to be quite brittle.
An end of the thin delaminated portion was easily snapped off with finger pressure.
The overall appearance of the piece, and it’s parent, strongly suggests rapid epitaxial growth.
A Jeol JSM - T330 SEM was used to examine portions of the smaller artifact fragment. Photos taken
showed features quite similar to those seen previously during recent analysis carried out at another midwestern
location. The layering effect is quite noticeable. Crystal structure of the light grey metal, composing the
thicker layers, is indeterminate visually. Original SEM photos taken at this location have been forwarded to LMH
for use with this summary.
III. Composition and Chemical Properties
A Tracor Northern 5400 EDS X ray analyzer was used to examine compositions of both silvery and
blackish regions. The silvery region is shown to be relatively pure Mg, with a small signal for Zn; perhaps
indicating about 2 to 3% of the latter. The blackish region appears to be primarily Bi. Please reference attached
EDS print-outs. Again, this corroborates results from earlier EDS and SIMS work done elsewhere.
A small crumb of the artifact was held by tweezers over a hydrogen torch flame. It ignited and
burned with the characteristic white flare of Mg. A small curl of 99.99% Mg was likewise ignited for comparison.
Both appeared to burn identically.
IV. Nuclear Properties
The larger artifact portion was tested with a Baird Atomic 914-434 Ratemeter (Geiger Counter). No
indications of radioactivity were noted.
Questions had been raised by LMH as to whether the materials in the artifact were of common
(predominant or stable) isotope. The only testing possible at this location for this purpose was a simple
Archimedian volume versus weight test. The volume of the large artifact portion was determined by displacement of
water in a pipette. Correcting for estimated volumes of Zn and Bi, a calculated weight was derived for the
artifact, given the textbook densities for Mg24 , Zn, and Bi. This value was calculated to be .5155g. The artifact
was then weighed with a Stanton CL1 lab balance, and actual weight over three trials was found to be .5115g, about
0.7% lighter than the calculated value. From this, we may say that the artifact, while possibly containing small
percentages of heavier Mg isotopes, does not appear to be primarily composed of Mg25 or Mg26.
V. Electrical Properties
The artifact appears to be quite conductive; and in any orientation, has a resistance too low to
measure with a typical ohm-meter.
A Fluke 79 DVM was used to look for any voltage potentials or currents which (by some hypotheses)
might be produced by the layering of dissimilar metals or other more unusual mechanisms. None were detected in the
range of the meter.
VI. Magnetic Properties
The artifact was tested with a custom - built Hall effect gaussmeter. No discernable magnetic
field was noted. The artifact was not seen to be attracted by a NdFeB magnet.
It had been suggested that the layered structure of the artifact resembled proposed structures for
high temperature filamentary superconductors. A small NdFeB super magnet was used in an attempt to elicit a
Meissner Effect reaction with the artifact, both at room temperature, and in a beaker of liquid nitrogen. No
effect was noticed.
VII. Testing for Unusual Properties
The artifact was radiated with light from a .5mW 670nm diode laser, at various angles. No unusual
effects or responses were noted.
The artifact was radiated with light from a 100watt long wave ultraviolet lamp. No fluorescence or
unusual response was noted.
The artifact was suspended within an electrical field of about 3 to 4 kV at 20 kHz. No unusual
responses were noted.
It had been suggested to LMH that the artifact structure was possibly indicative of a hypothetical
propulsion system, and that extremely high DC potentials applied to the metal structure would cause it to lose
weight! To test this idea, the artifact was mounted on a plastic stand, which in turn was placed on a Mettler
BasBal 2400 digital lab balance. A very thin lead wire was attached to the artifact with a snippet of conductive
tape, and then connected to a HV source. Two sources were used, a +/- 15,000V DC, 60VA supply (GE 9T63Y2226G2) and
a small Van De Graaf generator providing about 30 to 50 kV electrostatic potential.
In either case, no weight changes within the resolution of the balance (10mg) were noted when the
HV sources were turned on. However, according to LMH’s source, potentials over 1MV might be needed to cause weight
loss (?!).
VIII. Conclusions
At the most basic of levels, we would freely state that the artifact portion provided by LMH does
NOT seem to be composed of elements or compounds which are unknown. Nor is it composed of alloys that appear to be
of a purity or combination beyond the scope of current material science. The artifact bears a strong resemblance
to irregular layered residue often found in large physical vapor deposition (PVD) coaters. This family of filming
processes includes sputtering, E-beam, and resistively heated thermal evaporation; all common vacuum processes
used widely in industry. The structure of the artifact very strongly suggests long term, high rate, disordered
epitaxial growth on a cold surface (chilled evaporant shield? chamber walls?).
I have spent nearly 12 years working in the thin film and vacuum process fields. Some years ago,
I worked as a technician for a company in Ohio that ran the world’s largest commercial E-beam coater. One of my
duties was to remove chromium residue from the areas around the large E-beam evaporation sources. Hundreds of
pounds of chips, flakes, and chunks of columnar layered chromium residue were removed at a time. (Usually
weekends - third shift!) If I had not known the composition of the artifact when first viewing the colour photos
of it, I would have honestly guessed that someone had done me the honor of saving a souvenir from my old job - a
chrome residue chunk from the focus magnet pole piece of an Airco Temescal E-beam source! Rough calculations,
coupled with past work experience would hint that residues of the thickness of the artifact represent 80 to 120
hours of build up time, in your typical large sputter or E-beam coater. We used to chip ours out every two weeks
or so.
The composition of the Mg:Zn alloy comes close to several commercial Mg alloys: ASTM#’s ZK60A,
ZK51A, and EZ33A. All of these alloys, however, are said to have a very small quantity of Zr, typically 0.5% to
0.7%. I have been informed that Zr was not seen in earlier EDS scans at other locations, nor did it seem to be
evident in my analysis of the artifact. However, I do also know that at least for our TN 5400, resolution below
about 1% is usually not possible. Zr may have simply been below the resolution of the EDS. (Information from The
Mechanical Engineers Handbook, 1958 edition, McGraw Hill Book Co.)
It is also evident that the artifact does not, at least in it’s current state of condition, seem
to produce any voltages or currents, nor does it act as a superconductor, at least at room temperature or at
77K.
The remaining unusual aspect of the artifact is quite simply the combination of Mg and Bi in a
single structure. Mg, of course, finds most use in the automotive and aerospace industry, as a lighter weight
substitute for aluminum. It may also be used to make some optical grade films or plating. Bi, on the other hand,
has several unusual properties that suit it to more specialized high tech applications. It is often a component in
solders and is added to some lower temperature cast-able alloys because it has the characteristic of expanding
about 2 to 3 percent upon cooling. It is used in thermoelectric power modules or Peltier coolers along with
tellurium. It is the most diamagnetic element known, and the most electro-negative. A patent by Carroll claims Bi
as a possible filamentary superconductor at high temperatures. Bi is itself super-conducting at low
temperatures.
To date, I have been unable to find any references to uses of Mg and Bi together in one process
or product! LMH has claimed that officials at Dow, one of the largest Mg producers in the world, are unaware of
any use of Bi in their manufacturing processes.
Of course, this is not to say that there is not some very specialized use of Mg in a Bi
application, or vica versa, we have simply not found it yet in our "detective work".
My own opinion is that the artifact probably represents a curious piece of industrial by-product
from the thin films industry or a Mg casting plant. However, until a match-up is found, I will not rule out the
possibility of a more unusual origin.
Notes, as of November 2001:
In the year or so that followed the analysis by us of this sample, the mythos and mystery of the
bismuth - magnesium artifact continued to grow. It became the source for a wide range of speculations, some valid,
some baseless, among the anti-gravity and UFO research sub-cultures. The extraterrestrial origin of the artifact
appeared to be firmly entrenched in the minds of most who listened, read, and believed. Presumably, there just
aren't very many old films and vacuum technology folks out there...
Claims were made by a Tesla coil enthusiast in Alabama that the portion of the artifact in his
possession acted strangely and tried to levitate in the presence of the electrostatic field of a Van de Graaf
generator and a radio frequency source. We did perform a separate replication here, and found that our metal
fragment danced about as well in the field of a Van de Graaf. And so did a piece of aluminum foil! Please
understand that just about any small unattached mass will dance in the field of a 200,000 volt source! The mythos
grew...
In 2000, one last revelation came our way on the origin of the artifact. The combination of
bismuth and magnesium had eluded us for four years. But then one day, we found a reference to an obscure
industrial process used in the refinement of lead. The process, called the Betterton-Krohl Process, uses molten
magnesium floated over the surface of liquid lead. The magnesium sucks up, or pulls bismuth impurities out of the
lead! Often, the magnesium is used over and over again...
Could this little known process have been the real origin of some unusual looking metal residue,
that was then in turn promoted as a piece of alien technology?
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